Discussion Category:  Differential Scanning Calorimetry

Calibration

Dear sir,

We have your instrument DSC-60 and During Calibration One calibration parameter i.e. Sensitivity Test did not meet the acceptance criteria.

Test Parameter

Observed Value of current PM result

Limit

Sensitivity Test (Indium)

Onset Value

155.52 °C

154.9 to 157.9 °C

Enthalpy

-35.0 J/g 

-27.0 to -30.0 J/g

and root cause given that due  to improper sample preparation (improper crimping the sample crucible) during heat flow calibration and wrong factor was    calculated by the DSC-60t.Please provide scientific justification how it corelates each other.

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Asked by

Alka
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avatar placemarkReply by
m ezzat

hi alka

what your openion about shmadzu DSC 60 plus ?

i will buy it

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