Discussion Category: GC Systems
Front Inlet Septum Purge Shutdown
After initiating the method, the GC septum purge flow refuse to attain its set point of 3ml/min. Septum Purge flow remain stagnant on 0.1ml/min without increasing any further, and eventually shutdown after a few minutes.
Please what could be wrong?
Please find below the set points for my GC with the actual (current) readings indicated in parenthesis.
Front Inlet Parameter
Mode= split;
Temp = 150 degC;
Pressure= 23.97 psi;
Split ratio= 10;
Split flow= 34.69ml/min (actual= 37.56)
Septum purge = 3ml/min (actual= 0.1ml/min)
Gas saver ON
Saver flow =20 ml/min
Saver time = 2 mins
Note that when i disable the septum purge, the GC does not shutdown but as soon as i put the septum purge ON, the GC shutdown in safe mode.